The Microscope
Using the gemmological microscope for inclusion study, illumination techniques, and immersion methods to identify gems and detect treatments.
Introduction
The gemmological microscope is essential for studying inclusions, growth features,
and signs of treatment. Magnifications from 10× to 60× are typically used, with
various illumination techniques revealing different internal features.
Microscopy skills are fundamental to separating natural from synthetic gems and
detecting many treatments.
Microscope Types
Several microscope configurations are used in gemmology:
Stereo Microscope
The standard gemmological microscope:
- Binocular viewing: Comfortable, natural depth perception
- Variable magnification: Usually 10× to 45×
- Working distance: Adequate space for manipulation
- Various illumination options: Darkfield, brightfield, fibre-optic
Compound Microscope
Higher magnification for detailed work:
- Higher power: 100× to 400×
- Thinner depth of field: More difficult to use
- Specific applications: Examining very fine inclusions
- Not standard for routine gemmology
Magnification Ranges
Different magnifications serve different purposes:
| Magnification | Application | Notes |
|---|---|---|
| 10× | Standard loupe magnification; overview examination | FGA/GIA grading standard |
| 20× | General inclusion observation | Good balance of magnification and field |
| 30-40× | Detailed inclusion study | Most routine microscopy |
| 50-60× | Fine details, surface features | Reduced field of view |
| 100×+ | Specific investigations | Rarely needed; difficult to use |
Illumination Techniques
Different lighting reveals different features:
| Technique | Description | Best For |
|---|---|---|
| Darkfield | Light from sides; inclusions bright against dark background | Most inclusions, three-phase, silk |
| Brightfield | Light from below; transmitted through gem | Colour zoning, growth patterns, fingerprints |
| Fibre-optic | Directed beam for pinpoint illumination | Individual inclusions, surface features |
| Overhead | Reflected light from above | Surface features, coatings, wear |
| Polarised | Light through crossed polars | Strain, twinning, birefringence |
Darkfield Illumination
The most commonly used technique:
How It Works
Light enters from the sides rather than directly below:
- Background appears dark
- Inclusions scatter light and appear bright
- Excellent contrast for most internal features
- Standard setup for routine examination
What It Reveals
- Crystal inclusions (bright points or shapes)
- Silk and needle inclusions
- Gas bubbles
- Fractures and feathers
- Fingerprints (healed fractures)
- Three-phase inclusions
Brightfield and Other Techniques
Alternative illumination for specific observations:
Brightfield
Light transmitted directly through the stone:
- Colour zoning: Visible as bands or areas of different colour
- Growth patterns: Hexagonal zoning in corundum
- Colour concentration: Around fractures or surfaces
- Best for: Transparent stones with colour variations
Fibre-Optic Illumination
Directed light for specific features:
- Pinpoint individual inclusions
- Trace fractures and feathers
- Examine drill holes
- Light difficult-to-reach areas
Oblique and Shadow Illumination
Light at steep angles:
- Enhances surface texture
- Reveals polish quality
- Shows surface-reaching features
- Highlights laser drill holes
Immersion Technique
Immersing the gem in a liquid of similar RI reduces surface reflections and reveals
internal features more clearly.
Common Immersion Liquids
| Liquid | RI | Best For | Safety Notes |
|---|---|---|---|
| Water | 1.33 | Basic immersion; safe for all gems | Safe |
| Benzyl benzoate | 1.57 | Quartz, beryl, feldspar | Low toxicity |
| Methylene iodide | 1.74 | Corundum, spinel, garnet | Toxic; handle with care |
| Clove oil | 1.54 | General purpose | Pleasant odour; low toxicity |
Immersion Observations
Immersion reveals:
- Colour zoning: Much clearer than in air
- Growth patterns: Curved (synthetic) vs angular (natural)
- Surface treatments: Diffusion layers
- Internal features: Without surface reflections
Immersion Warning
Diagnostic Inclusions
Certain inclusions are diagnostic for species or origin:
By Gem Species
| Gem | Characteristic Inclusions |
|---|---|
| Corundum | Silk (rutile needles), fingerprints, hexagonal zoning |
| Emerald | Three-phase inclusions (Colombian), jardín, calcite |
| Spinel | Octahedral crystals, fingerprints, often cleaner than corundum |
| Tourmaline | Growth tubes, needles, colour zoning |
| Peridot | Lily pads (stress discs around chromite) |
| Topaz | Two-phase inclusions, growth tubes |
Natural vs Synthetic
Key differences to look for:
- Natural: Irregular growth, natural crystal inclusions
- Flame fusion: Gas bubbles, curved striae
- Flux synthetic: Flux inclusions, platinum crystals
- Hydrothermal: Seed plate, chevron patterns
Treatment Detection
The microscope is essential for treatment detection:
- Heat treatment: Altered silk, stress fractures, melted inclusions
- Fracture filling: Flash effect, gas bubbles in filler
- Lead glass filling: Flash effect, trapped bubbles
- Beryllium diffusion: Colour concentration at facet junctions
- Laser drilling: Thin tubes reaching inclusions
- Coating: Iridescence, colour concentration at surface